1.1 Grinding with a Cutting Mill (Wiley or equivalent)
Safety Precautions:
- Wear a dust mask and avoid inhaling dust.
- Do not insert fingers or objects into the grinding mill.
- Observe all safety and operating instructions supplied by
the manufacturer.
Procedure:
- Inspect the mill for cleanliness.
- Insert the appropriate screen into the mill. If a fine
grind is desired, most samples are ground with the 1 mm
screen. If large samples are to be ground, it may be
faster to grind them using a 4 to 6 mm screen and then
regrind using the 1 mm screen.
- Latch the door in place. Do not overtighten to avoid the
rotor binding against the door.
- Insert the sample receiving container into place.
- Close the feeding gate at the top of the mill.
- Turn on the switch.
- Add sample to the feeding chute. Partially open the
feeding gate to allow sample to enter, then shut the
gate. If necessary, push sample into the mill with a
spatula or wooden plunger with stop to prevent entry into
grinder knives.
- After the first portion has been ground (listen for the
"empty" higher pitched sound), feed another
portion into the mill.
- Allow the mill to run for at least two min after the last
portion has been added to ensure that the entire sample
has passed through. Listen for the "empty"
higher pitched sound, then shut off switch.
- Hold the sample container beneath the grinding chamber
and open the mill. Use a brush or spatula to transfer
incompletely-ground residue from mill to the container
with ground sample. Remove the screen and transfer
residue from it into the sample container.
- Clean the entire mill using air and/or a brush. A fine,
pointed spatula works best to dislodge particles caught
behind the knives. The mill may need washing with certain
samples. Towel dry or blow dry to prevent rust formation.
Comments:
- The knives need periodic sharpening. Proper alignment of
the knives on re-installation is critical to ensure
efficient grinding.
- Dust will accumulate in the motor housing compartment and
should to be cleaned out periodically.
- Condition of mill, maintenance and repairs should be
monitored and regularly recorded in a designated log
book.
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